係幉宆帺摦夞愜寁棙梡偺庤堷偒
2003/05/14
倃慄寢徎峔憿夝愅幚尡巤愝塣塩埾堳夛
1丏係幉宆帺摦夞愜寁傪巊梡偡傞偵偁偨偭偰
丂杮憰抲偼丄X慄寢徎峔憿夝愅幚尡巤愝塣塩埾堳夛 (塸柤丗Committee for X-ray
crystallography laboratory at Tokyo University of Agriculture & Technology)
(埲壓塣塩埾堳夛) 偑娗棟偟偰偄傑偡丅巊梡偵偁偨偭偰偼埲壓偺帠崁傪弲庣丒偛椆夝偔偩偝偄丅
侾丏倃慄幒偵偍偄偰幚尡偡傞幰偼丄奺晹嬊偵偍偄偰曻幩慄庢埖幰偺搊榐傪峴偄丄擖幒偵嵺偟偰偼僼傿儖儉僶僢僠傪拝梡偟偰壓偝偄丅
俀丏巊梡偵摉偨偭偰偼丄偙偺庤堷彂傪弉撉偺忋丄廫暘偵棟夝丒弲庣偟偰偔偩偝偄丅
俁丏應掕拞偼丄昁偢枅擔丄憰抲偺條巕傪尒偵棃傞傛偆偵偟偰壓偝偄丅
係丏倃慄幒偺弌擖傝偼丄尨懃偲偟偰丄廽媥擔傪彍偔寧梛擔偐傜嬥梛擔丄9:00~19:00 偱偡丅
丂廡偺恀拞偵媥擔偑棃傞廡偼偱偒傞偩偗旔偗偰梊栺傪庢偭偰偔偩偝偄丅
俆丏杮憰抲偵傛傞惉壥傪榑暥偱敪昞偝傟傞応崌偼丄杮憰抲傪巊梡偟偨巪丄榑暥偵柧婰偟丄暿嶞傪堦晹丄塣塩埾堳夛埾堳挿傑偱偍憲傝偔偩偝偄丅埲壓偵椺傪俀偮嫇偘傑偡丅
Diffraction data were
measured on a Rigaku AFC7R diffractometer at the X-ray crystallography
laboratory,
We are indebted to the
X-ray crystallography laboratory at
俉丏憰抲巊梡拞偵堎忢傪姶偠偨傜偡偖偵埲壓偺僔僗僥儉娗棟幰傑偱楢棈偟偰壓偝偄丅
丂丂楢棈愭丗丂擾妛晹墳梡惗暔壢妛壢丂揳捤棽巎丂撪慄 (5702)
俀丏寢徎傪庢傝晅偗傞
丂丂丂丂丂丂丂戝婥拞偱寢徎偑埨掕側応崌
侾丏嬥懏惢偺僺儞 (儐乕僓乕偵偼 俆 杮戄梌偟傑偡) 偵丄嵶偄僈儔僗朹傪愙拝嵻偱晅偗傞丅
丂丂愙拝嵻偑屌壔偟偨傜丄壓偵帵偡傛偆側挿偝偵僈儔僗朹傪愗抐偡傞丅
俀丏尠旝嬀壓偱寢徎傪僈儔僗朹偺愭偵晅偗傞丅
丂丂丂丂丂丂丂丂丂丂丂丂戝婥拞偱寢徎偑晄埨掕側応崌(僞儞僷僋幙摍)
侾丏巗斕偺僈儔僗僉儍僺儔儕乕偵寢徎曣塼偲偲傕偵晻擖偡傞丅偙偺応崌丄僺儞偺僿僢僪偲寢徎偲偺嫍棧偼僈儔僗朹偵庢傝晅偗傞応崌偲摨偠偱偁傞丅
丂丂丂丂丂丂丂丂丂丂丂丂丂丂丂丂丂丂
丂丂丂丂丂丂丂丂丂丂丂丂丂丂俁丏梊栺傪偲傞
巊梡慜偵擾妛晹偺揳捤丂撪慄乮5704乯丄儊乕儖tonozuka (at-mark) cc.jskrtf.com傑偱楢棈偟偰偔偩偝偄丅
丂丂丂丂丂丂丂丂丂丂丂丂丂丂係丏幚尡傪偡傞慜偵
侾丏X慄幒偺僪傾偵嵼幒偺尞傪妡偗傞丅婣戭偡傞偲偒偼嶥傪倃慄幒撪傊栠偟偰偍偔丅
俀丏旛偊晅偗偺巊梡曤偵昁梫帠崁傪婰擖偡傞丅
丂丂丂丂丂丂丂丂丂丂丂丂丂丂俆丏X慄傪敪惗偝偣傞
侾丏X慄敪惗憰抲偺僷僱儖傪忋偵帵偡丅OPERATE嘆儔儞僾偑揰摂偟偰偄傞偙偲傪妋偐傔偰 POWER ON嘇儃僞儞傪墴偡丅
俀丏夋柺嘊偵 READ NOW 偺昞帵偑弌偨偙偲傪妋偐傔偰
XRAY ON嘋儃僞儞傪墴偡丅儔儞僾偑揰摂偟偰 20 kV, 10 mA 偺弌椡偱 X 慄偑敪惗偡傞丅 READ
NOW 偺昞帵偑弌側偄応崌丄偦偺尨場偲偟偰偼杊岇僇僶乕偺偳偙偐偑奐偄偰偄傞壜擻惈偑偁傞丅杊岇僇僶乕傪慡偰僠僃僢僋偟偰側偍偐偮 READ NOW 偺昞帵偑弌側偄応崌偼僔僗僥儉娗棟幰傑偱楢棈偡傞丅
俁丏MENU 儃僞儞偺嘍傪墴偟偰夋柺偵儊僯儏乕傪昞帵偝偣傞丅僇乕僜儖儃僞儞嘐傪墴偟偰 kV/mA SET 偺偲偙傠傑偱僇乕僜儖傪帩偭偰偄偒 ENTER 儃僞儞嘑傪墴偡丅kV/UP DN 儃僞儞嘒丄mA/UP DN 儃僞儞嘓傪巊梡偟偰埲壓偵帵偡傛偆偵X慄偺弌椡傪忋偘偰偄偔丅
|
kV |
20 |
20 |
20 |
30 |
30 |
30 |
36 |
36 |
40 |
40 |
50 |
50 |
|
mA |
10 |
50 |
100 |
50 |
100 |
200 |
100 |
200 |
100 |
200 |
100 |
200 |
|
帪娫(暘) |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
5 |
丂丂丂丂丂丂丂丂丂丂丂丂丂丂俇丏僨乕僞傪應掕偡傞
侾丏係幉帺摦夞愜寁偺僐儞僩儘乕儔乕偺僗僀僢僠傪 ON 偵偡傞丅
俀丏PC 偺僗僀僢僠傪 ON 偵偡傞丅
俁丏CD 僐儅儞僪偱儐乕僓乕柤偺僨傿儗僋僩儕乕傊峴偔丅椺丗CD SAKANO
係丏GETMAS 偲擖椡偡傞丅
俆丏CTR 偲擖椡偡傞丅
俇丏ALLINIT 偲昞帵偝傟偰偄傞偙偲傪妋偐傔偰儕僞乕儞僉乕傪懪偮丅
俈丏偟偽傜偔偡傞偲僐儅儞僪擖椡忬懺偲側傞丅仜60 偲擖椡偡傞丅
俉丏X慄敪惗憰抲偺 DOOR 儃僞儞嘔傪墴偡丅僺乕僺乕偲偄偆壒偑側傝丄杊岇僇僶乕傪奐偗傞偙偲偑偱偒傞丅DOOR 儃僞儞傪墴偝偢偵杊岇僇僶乕傪奐偗傞偲X慄偑嬞媫掆巭偡傞偺偱拲堄偡傞丅
俋丏僑僯僆儊乕僞乕僿僢僪 (埲壓僑僯僆) 傪壓偵帵偡丅僑僯僆偼戝曄崅壙側偺偱偦偺庢傝埖偄偵偼嵶怱偺拲堄傪暐偆偙偲丅傑偢僱僕嘆傪彮偟娚傔偰 (娚傔偡偓傞偲奜傟偰偟傑偆偺偱拲堄偡傞)丄寢徎傪庢傝晅偗傞丅師偵僑僯僆傪係幉帺摦夞愜寁偵庢傝晅偗傞丅
丂丂丂
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侾侽丏僑僯僆偺僱僕嘇傪彮偟娚傔偰僱僕嘊傪夞偟丄尠旝嬀偱寢徎傪尒側偑傜戝懱偺崅偝傪挷愡偡傞丅
侾侾丏係幉帺摦夞愜寁偺僑僯僆庢傝晅偗埵抲偵偁傞僱僕(僑僯僆屌掕僱僕) 傪彮偟娚傔傞偲僑僯僆偑帺桼夞揮偱偒傞傛偆偵側傞偺偱丄忢偵夞揮幉忋偵寢徎偑偔傞傛偆偵僑僯僆偺僱僕嘋丄嘍傪夞偟偰挷惍偡傞丅朷墦嬀偺廫帤偑昁偢偟傕夞揮幉忋偲堦抳偟偰偄側偄偺偱拲堄偡傞丅
侾俀丏侾侽丆侾侾偺憖嶌傪孞傝曉偟偰挷惍偑廔傢傟偽丄PC 偐傜 C90 偲擖椡偟偰寢徎偺拞怱偺埵抲傪妎偊傞丅師偵 PC 偐傜 C-90 偲擖椡偟偰寢徎偺拞怱偺埵抲偑摨偠偱偁傞偙偲傪妋偐傔傞丅傕偟偢傟偰偄傟偽僑僯僆偺僱僕嘊偱挷惍偡傞丅
侾俁丏挷惍偑廔傢傟偽丄僑僯僆偺僱僕嘇偍傛傃係幉帺摦夞愜寁偺僑僯僆屌掕僱僕傪寉偔掲傔偰丄杊岇僇僶乕傪掲傔傞丅
侾係丏PC 偐傜 AUTO 偲擖椡偡傞丅夋柺弌椡傪僾儕儞僞乕偵弌椡偟偨偄応崌偼 PRINT ON 偵丄傑偨僼傽僀儖偵弌椡偟偨偄応崌偼 LIST 偵儅僂僗傪巊梡偟偰曄峏偡傞丅
丂丂丂丂丂丂丂丂丂丂丂丂丂丂俈丏應掕偑廔傢偭偨傜
侾丏EXIT 偲擖椡偟偰捠忢偺夋柺偵栠傞丅
俀丏PC 偐傜 PROCMENU 偲擖椡偡傞丅
俁丏巜帵偵廬偭偰僨乕僞傪擖椡偟偰偄偔丅傢偐傜側偄偲偙傠偼儕僞乕儞偱傛偄丅
係丏FTP CSASP 偲擖椡偡傞丅
俆丏login name
傪恥偄偰偔傞偺偱 pub 偲擖椡偡傞丅僷僗儚乕僪偼(丂丂丂丂丂丂)
俇丏ftp> 偺暥帤偑弌偨傜丄cd 僐儅儞僪偱儐乕僓乕柤偺僨傿儗僋僩儕乕傊峴偔丅
丂丂丂椺丗cd sakano
俈丏mput *.* 偲擖椡偡傞丅
俉丏quit 偲擖椡偡傞丅
俋丏shut down 偲擖椡偡傞丅
侾侽丏PC 偺僗僀僢僠傪 OFF 偵偡傞丅僾儕儞僞乕傪巊梡偟偨応崌僾儕儞僞乕僗僀僢僠傪 OFF 偵偟偰丄帺暘偱巊偭偨弌椡梡巻偼帩偪婣傞丅
侾侾丏係幉帺摦夞愜寁偺僐儞僩儘乕儔乕偺僗僀僢僠傪 OFF 偵偡傞丅
侾俀丏僑僯僆儊乕僞乕僿僢僪傪係幉帺摦夞愜寁偐傜庢傝奜偟丄寢徎傪僑僯僆儊乕僞乕僿僢僪偐傜庢傝奜偡丅寢徎丄偦偺懠帩偪崬傫偩傕偺偼昁偢帩偪婣傞偙偲丅
侾俁丏X慄偺弌椡傪埲壓偵廬偭偰 20 kV丄10 mA 傑偱壓偘傞丅
|
kV |
50 |
40 |
36 |
30 |
30 |
20 |
20 |
|
mA |
100 |
100 |
100 |
100 |
50 |
50 |
10 |
|
帪娫(暘) |
10 |
10 |
10 |
10 |
10 |
10 |
10 |
侾係丏XRAY 僗僀僢僠傪 OFF 偵偡傞丅POWER 僗僀僢僠傪 OFF 偵偡傞丅
侾俆丏僨乕僞偑 CSASP 偵揮憲偝傟偰偄傞偙偲傪妋偐傔偨屻丄昁偢 PC 偺帺暘偺僨傿儗僋僩儕乕撪偺僨乕僞偼 DEL 僐儅儞僪偱徚嫀偟偰偍偔偙偲丅
丂丂丂丂丂丂丂丂丂丂丂丂丂丂俉丏峔憿夝愅
侾丏僐儞僺儏乕僞偵 login 偡傞丅
俀丏PC 偐傜僨乕僞傪揮憲偟偨僨傿儗僋僩儕乕傊峴偔丅
俁丏texsan 偲擖椡偡傞丅
係丏process raw data
俆丏solve